
ACE Experimental Record


Inlet Method File: c:\masslynx\projects\csf_mtg.pro\acqudb\nt

---------------------   Run method parameters   ----------------

-- PUMP --

Waters Acquity SDS
 Run Time: 3.00 min
 Comment:  
 Solvent Selection A: A1 
 Solvent Selection B: B2 
 Low Pressure Limit: 0.000 psi
 High Pressure Limit: 15000.000 psi
 Solvent Name A: 0.1% FA in Water 
 Solvent Name B: Methanol 
 Switch 1: No Change 
 Switch 2: No Change 
 Switch 3: No Change 
 Seal Wash: 4.5 min
 Chart Out 1: System Pressure 
 Chart Out 2: %B 
 System Pressure Data Channel: No 
 Flow Rate Data Channel: No 
 %A Data Channel: No 
 %B Data Channel: No 
 Primary A Pressure Data Channel: No 
 Accumulator A Pressure Data Channel: No 
 Primary B Pressure Data Channel: No 
 Accumulator B Pressure Data Channel: No 
 Degasser Pressure Data Channel: No 
 [Gradient Table]
  Time(min) Flow Rate(mL/min) %A %B Curve 
 1. Initial 0.350 95.0 5.0 Initial 
 2. 0.80 0.350 95.0 5.0 6 
 3. 1.50 0.350 75.0 25.0 6 
 4. 2.50 0.350 75.0 25.0 6 
 5. 2.60 0.350 95.0 5.0 6 
 6. 3.00 0.350 95.0 5.0 1 
 Run Events: Yes 
 Gradient Start (Relative to Injection): 0 uL
 2D Repeat: No 

-- END PUMP --

-- AUTOSAMPLER --

Waters Acquity AutoSampler 
 Run Time: 3.00 min
 Comment:  
 Load Ahead: Disabled 
 Injection Mode: Partial Loop With Needle Overfill 
 LoopOffline: Disable 
 Weak Wash Solvent Name:  
 Weak Wash Volume: 1000 uL
 Strong Wash Solvent Name:  
 Strong Wash Volume: 500 uL
 Target Column Temperature: 35.0 °C
 Column Temperature Alarm Band: Disabled 
 Target Sample Temperature: 10.0 °C
 Sample Temperature Alarm Band: Disabled 
 Full Loop Overfill Factor: Automatic 
 Syringe Draw Rate: Automatic 
 Needle Placement: Automatic 
 Pre-Aspirate Air Gap: Automatic 
 Post-Aspirate Air Gap: Automatic 
 Column Temperature Data Channel: No 
 Ambient Temperature Data Channel: No 
 Sample Temperature Data Channel: No 
 Sample Organizer Temperature Data Channel: No 
 Sample Pressure Data Channel: No 
 Preheater Data Channel: No 
 Switch 1: No Change 
 Switch 2: No Change 
 Switch 3: No Change 
 Switch 4: No Change 
 Chart Out: Sample Pressure 
 Sample Temp Alarm: Disabled 
 Column Temp Alarm: Disabled 
 Run Events: Yes 
 Needle Overfill Flush: Automatic 
 No Injection: No 
 Active Preheater: Enabled 


Sample Run Injection Parameter

Injection Volume (ul)   -   1.00
-- END AUTOSAMPLER --

----------------------------  oOo  -----------------------------


End of experimental record.

------------------- Waters Acquity SM Postrun Report  ---------------




 Software Version: 1.73.4159 

 Firmware Version: 1.70.392 (Sep 28 2017) 

 Checksum: 0x30b5761d 

 Serial Number: A19FLP193M 

 Sample Syringe Size: 100.0 

 Sample Loop Size: 10.0 

 Needle Size: 10.0 

 Column Type: ACQUITY UPLC® HSS T3 1.8µm 

 Column Serial Number: 02693204115169 

 Total Injections on Column: 2691 

 Auto-defrost Enabled: Yes 

 Minimum Sample Temperature: 10.0 

 Maximum Sample Temperature: 10.0 

 Average Sample Temperature: 10.0 

 Minimum Column Temperature: 40.2 

 Maximum Column Temperature: 42.0 

 Average Column Temperature: 41.1 

 Measured Loop Volume: 0.000 

 Measured Loop Volume No Pressure: 0.000 


----------------------------  oOo  -----------------------------





------------------- Waters Acquity SDS Postrun Report  ---------------




 Software Version: 1.73.3499 

 Firmware Version: 1.73.423 (Apr 14 2020) 

 Checksum: 0x191bbcbf 

 Serial Number: B19BSP149G 

 Minimum System Pressure: 6506.7 

 Maximum System Pressure: 7316.0 

 Average System Pressure: 6888.0 

 Minimum Degasser Pressure: 0.5 

 Maximum Degasser Pressure: 0.5 

 Average Degasser Pressure: 0.5 

 User Set Maximum Pressure: 18000 


----------------------------  oOo  -----------------------------

